di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

Base Information

Chemical Name:di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate
CAS No.:1099752-56-3
Molecular Formula:C₃₄H₄₁NO₅
Molecular Weight:543.703
Hs Code.:

Synonyms:di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

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Technology Process of di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

There total 2 articles about di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1087136-71-7
methyl (E)-5-(trityloxy)pent-2-en-1-yl carbonate

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 1099752-56-3
di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; triethylamine; (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-[(1S)-1-(2-methoxy-phenyl)ethyl]amine; In tetrahydrofuran; at 20 ℃; for 3h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0028-1083158

Reference yield:

: 1087136-71-7
methyl (E)-5-(trityloxy)pent-2-en-1-yl carbonate

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 1099752-56-3
di-tert-butyl (+)-{(1R)-[2-(trityloxy)ethyl]prop-2-enyl}imidodicarbonate

: 1099752-66-5
di-tert-butyl [(2E)-5-(trityloxy)pent-2-enyl]imidodicarbonate

Guidance literature:: With O,O'-((S)-1,1'-binaphthyl-2,2'-diyl)-N,N'-di-(S,S)-(1-naphthalen-1-yl)-ethyl-phosphoramidite; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; triethylamine; In tetrahydrofuran; at 20 ℃; for 6h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0028-1083158