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2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene

Base Information
  • Chemical Name:2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene
  • CAS No.:1160518-30-8
  • Molecular Formula:C25H37N
  • Molecular Weight:351.575
  • Hs Code.:
2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene

Synonyms:2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene

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Chemical Property of 2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene
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Technology Process of 2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene

There total 1 articles about 2-(2,6-diisopropylphenyl)-3,3,6,8-tetramethyl-2-azaspiro[4,5]dec-7-ene-1-ylidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium diisopropyl amide; In diethyl ether; at -78 - 20 ℃; Inert atmosphere;
Guidance literature:
In tetrahydrofuran; (Ar); addn. of THF soln. of carbene deriv. to THF soln. of gold compd., stiring at room temp. for 12 h in dark; evapn., washing with hexane, extn. (CH2Cl2), evapn., NMR and MS;
Guidance literature:
In tetrahydrofuran; at -78 - 20 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.5b05868
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