N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

Base Information

Chemical Name:N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside
CAS No.:103216-93-9
Molecular Formula:C₁₈H₂₅NO₈S₂
Molecular Weight:447.53
Hs Code.:

Synonyms:N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

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Technology Process of N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

There total 4 articles about N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 103216-91-7
N-acetyl-p-aminophenyl 2,3-di-O-benzoyl-4-S-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-1,4-dithio-β-D-xylopyranoside

: 103216-93-9
N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

Guidance literature:: With sodium methylate; In methanol; for 24h;
DOI:10.1016/0008-6215(85)85004-7

Reference yield:

: 82040-50-4
1,2,3-tri-O-benzoyl-4-S-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-4-thio-α-D-xylopyranose

: 103216-93-9
N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: HBr / acetic acid; CH₂Cl₂ / 1 h / Ambient temperature

2: K₂CO₃ / acetone / 1 h / Ambient temperature

3: 90 percent / pyridine / 12 h / Ambient temperature

4: 90 percent / sodium methoxide / methanol / 24 h

With hydrogen bromide; sodium methylate; potassium carbonate; In pyridine; methanol; dichloromethane; acetic acid; acetone;
DOI:10.1016/0008-6215(85)85004-7

Reference yield:

: 82040-52-6
C₃₀H₃₁BrO₁₂S

: 103216-93-9
N-acetyl-p-aminophenyl 4-S-β-D-xylopyranosyl-1,4-dithio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / 1 h / Ambient temperature

2: 90 percent / pyridine / 12 h / Ambient temperature

3: 90 percent / sodium methoxide / methanol / 24 h

With sodium methylate; potassium carbonate; In pyridine; methanol; acetone;
DOI:10.1016/0008-6215(85)85004-7