dibenzophospholyl(diphenylphosphino)methane-borane

Base Information

Chemical Name:dibenzophospholyl(diphenylphosphino)methane-borane
CAS No.:1193320-52-3
Molecular Formula:C₂₅H₂₃BP₂
Molecular Weight:396.216
Hs Code.:

Synonyms:dibenzophospholyl(diphenylphosphino)methane-borane

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Chemical Property of dibenzophospholyl(diphenylphosphino)methane-borane

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Technology Process of dibenzophospholyl(diphenylphosphino)methane-borane

There total 2 articles about dibenzophospholyl(diphenylphosphino)methane-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1088-00-2
9-phenyl-9-phosphafluorene

: 1013636-16-2
(chloromethyl)diphenylphosphine-borane

: 1193320-52-3
dibenzophospholyl(diphenylphosphino)methane-borane

Guidance literature:: 9-phenyl-9-phosphafluorene; With lithium; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;

With aluminum (III) chloride; In tetrahydrofuran; at -20 - 0 ℃; for 0.5h; Inert atmosphere;

(chloromethyl)diphenylphosphine-borane; In tetrahydrofuran; at -78 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/om2008265

Reference yield: 52.0%

: 1013636-16-2
(chloromethyl)diphenylphosphine-borane

: 70703-24-1
lithium dibenzophospholyl

: 1193320-52-3
dibenzophospholyl(diphenylphosphino)methane-borane

Guidance literature:: With Pd(OAc)2; [(Ph₂PC₅H₄)2Fe]; In tetrahydrofuran; (Ar); soln. of B compd. in THF was added to soln. of Li compd. in THF at-78°C; soln. of Pd salt and Fe complex in THF was added; stirred for 48 h; concd.; quenched with H2O; extd. (CH2Cl2); dried (MgSO4); evapd.; chromd. (silica gel, CH2Cl2/hexane, 50/50 or 40/60); elem. anal.;
DOI:10.1021/om900684w