Technology Process of C20H26N2O5S
There total 5 articles about C20H26N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium dichromate (PDC), MgSO4 / CH2Cl2 / 51 h
2: 65 percent / methanol / 18 h / Heating
3: 54 g / methanol / 17 h
With
dipyridinium dichromate; magnesium sulfate;
In
methanol; dichloromethane;
DOI:10.1021/ja00058a011
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 84 g / cerium trichloride heptahydrate, NaBH4 / methanol / 0.25 h
2: 80 g / MCPBA, sodium bicarbonate / CH2Cl2 / 0.67 h
3: pyridinium dichromate (PDC), MgSO4 / CH2Cl2 / 51 h
4: 65 percent / methanol / 18 h / Heating
5: 54 g / methanol / 17 h
With
sodium tetrahydroborate; dipyridinium dichromate; cerium(III) chloride; sodium hydrogencarbonate; magnesium sulfate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane;
DOI:10.1021/ja00058a011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 g / MCPBA, sodium bicarbonate / CH2Cl2 / 0.67 h
2: pyridinium dichromate (PDC), MgSO4 / CH2Cl2 / 51 h
3: 65 percent / methanol / 18 h / Heating
4: 54 g / methanol / 17 h
With
dipyridinium dichromate; sodium hydrogencarbonate; magnesium sulfate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane;
DOI:10.1021/ja00058a011
