(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Base Information

Chemical Name:(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester
CAS No.:499131-29-2
Molecular Formula:C₁₅H₂₂O₅S
Molecular Weight:314.403
Hs Code.:

Synonyms:(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Suppliers and Price of (R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

There total 4 articles about (R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 627-67-8
1-nitro-3-methylbutane

: 499131-29-2
(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran / 1 h / -95 - -90 °C

1.2: tetrahydrofuran / 1 h / -95 - -90 °C

2.1: Pd(OAc)2 / 168 h / Heating

3.1: 273.5 mg / diethyl ether

With n-butyllithium; palladium diacetate; In tetrahydrofuran; diethyl ether; 1.2: Michael addition / 2.1: Meyer reaction;
DOI:10.1055/s-2002-34368

Reference yield:

: 412021-12-6
Phenyl-methanesulfonic acid (3aR,5R,6R,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

: 499131-29-2
(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran / 1 h / -95 - -90 °C

1.2: tetrahydrofuran / 1 h / -95 - -90 °C

2.1: Pd(OAc)2 / 168 h / Heating

3.1: 273.5 mg / diethyl ether

With n-butyllithium; palladium diacetate; In tetrahydrofuran; diethyl ether; 1.2: Michael addition / 2.1: Meyer reaction;
DOI:10.1055/s-2002-34368

Reference yield:

: 412021-26-2
(1R,2R)-3-Methyl-2-nitromethyl-1-phenyl-butane-1-sulfonic acid (3aR,5R,6R,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

: 499131-29-2
(R,R)-2-(1-methoxysulfonyl-1-phenylmethyl)-3-methylbutyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / 48 h / Heating

2: diethyl ether

With trifluoroacetic acid; In diethyl ether; 1: Meyer reaction;
DOI:10.1055/s-2005-872164