C₂₄H₂₂BrN₃O₄

Base Information

Chemical Name:C₂₄H₂₂BrN₃O₄
CAS No.:1332848-38-0
Molecular Formula:C₂₄H₂₂BrN₃O₄
Molecular Weight:496.36
Hs Code.:

C<sub>24</sub>H<sub>22</sub>BrN<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₂BrN₃O₄

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Chemical Property of C₂₄H₂₂BrN₃O₄

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Technology Process of C₂₄H₂₂BrN₃O₄

There total 2 articles about C₂₄H₂₂BrN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.1%

: 1332848-36-8
C₂₄H₂₃N₃O₄

: 1332848-38-0
C₂₄H₂₂BrN₃O₄

Guidance literature:: With pyridinium hydrobromide perbromide; In 2,2,2-trifluoroethanol; at 23 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja206743v

Reference yield:

: 1116188-99-8
Nα-Boc-N1-Cbz-L-tryptophan methyl ester

: 1332848-38-0
C₂₄H₂₂BrN₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 23 °C / Inert atmosphere

1.2: 3.25 h / 0 - 23 °C / Inert atmosphere

2.1: pyridinium hydrobromide perbromide / 2,2,2-trifluoroethanol / 1 h / 23 °C / Inert atmosphere

With pyridinium hydrobromide perbromide; trifluoroacetic acid; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1021/ja206743v

Reference yield: 49.8%

: K[F₃BC₈H₄N(Cbz)CH₂C₇H₉N₂O₂]

: 1332848-38-0
C₂₄H₂₂BrN₃O₄

: 1332848-42-6
C₄₈H₄₄N₆O₈

Guidance literature:: With silver hexafluoroantimonate; 18-crown-6 ether; In Nitroethane; at 23 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja206743v