1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

Base Information

Chemical Name:1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol
CAS No.:1233956-74-5
Molecular Formula:C₅₀H₅₁NO₈
Molecular Weight:793.957
Hs Code.:

Synonyms:1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

Chemical Property:

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Technology Process of 1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

There total 3 articles about 1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1233956-73-4
C₄₂H₄₅NO₆

: 501-53-1,94274-21-2
benzyl chloroformate

: 1233956-74-5
1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

Guidance literature:: With potassium carbonate; In 1,4-dioxane; water; for 1h; Inert atmosphere;
DOI:10.1039/b9nj00629j

Reference yield:

: 1-D-1-O-(4-methoxybenzyl)-3,4,5,6-tetra-O-benzyl-scyllo-inosose

: 1233956-74-5
1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; sodium cyanoborohydride / tetrahydrofuran / 2 h / 20 °C

2: potassium carbonate / 1,4-dioxane; water / 1 h / Inert atmosphere

With ammonium acetate; sodium cyanoborohydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1039/b9nj00629j

Reference yield:

: 170900-81-9
3,4,5,6-tetra-O-benzyl-1-O-p-methoxybenzyl-D-myo-inositol

: 1233956-74-5
1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride; dimethyl sulfoxide / 14 h / 20 °C / Inert atmosphere

2: ammonium acetate; sodium cyanoborohydride / tetrahydrofuran / 2 h / 20 °C

3: potassium carbonate / 1,4-dioxane; water / 1 h / Inert atmosphere

With ammonium acetate; acetic anhydride; sodium cyanoborohydride; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; 1,4-dioxane; water; 1: Swern oxidation;
DOI:10.1039/b9nj00629j