3-phenylpropanoic thioanhydride

Base Information

• Chemical Name: 3-phenylpropanoic thioanhydride
• CAS No.: 1442466-49-0
• Molecular Formula: C₁₈H₁₈O₂S
• Molecular Weight: 298.406

Synonyms:3-phenylpropanoic thioanhydride

Chemical Property of 3-phenylpropanoic thioanhydride

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 3-phenylpropanoic thioanhydride

There total 1 articles about 3-phenylpropanoic thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

hydrocinnamic acid chloride (645-45-4) → 3-phenylpropanoic thioanhydride (1442466-49-0)

Guidance literature:

With Li⁽¹⁺⁾*AlH₄^(1-)*HS^(1-); In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1016/j.bmc.2013.02.053

Reference yield: 68.0%

3-phenylpropanoic thioanhydride (1442466-49-0) → 3-phenyl-N-(3-phenylpropanoyl)propanamide (1158-34-5)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.bmc.2013.02.053

upstream raw materials:

hydrocinnamic acid chloride

Downstream raw materials:

3-phenyl-N-(3-phenylpropanoyl)propanamide

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