(S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide

Base Information

• Chemical Name: (S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide
• CAS No.: 1380102-37-3
• Molecular Formula: C₁₈H₂₄F₂N₂O₂
• Molecular Weight: 338.398

Synonyms:(S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide

Chemical Property of (S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide

Chemical Property:

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Technology Process of (S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide

There total 1 articles about (S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

3,4-Difluorobenzoic acid (455-86-7) + 1-(2-cyclopentyl-2-(methylamino)ethyl)azetidin-3-ol dihydrochloride → (S)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide (1380102-37-3) + (R)-N-(1-cyclopentyl-2-(3-hydroxyazetidin-1-yl)ethyl)-3,4-difluoro-N-methylbenzamide (1380102-36-2)

Guidance literature:

3,4-Difluorobenzoic acid; 1-(2-cyclopentyl-2-(methylamino)ethyl)azetidin-3-ol dihydrochloride; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 3h;

With triethylamine; In ethanol; n-heptane; Resolution of racemate;

upstream raw materials:

3,4-Difluorobenzoic acid

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