methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

Base Information

Chemical Name:methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate
CAS No.:586344-24-3
Molecular Formula:C₂₁H₂₇N₃O₆
Molecular Weight:417.462
Hs Code.:

Synonyms:methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

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Chemical Property of methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

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Technology Process of methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

There total 3 articles about methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 2-(2-tert-butoxy-2-oxoethyl)-7-methoxycarbonyl-5-oxo-5,6,7,8-tetrahydroimidazo[1,5-c]pyrimidine-2-ium bromide

: 100-51-6,185532-71-2
benzyl alcohol

: 586344-24-3
methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 16h; Heating / reflux;

Reference yield:

: 69614-04-6
S-(+)-7-Methoxycarbonyl-5,6,7,8-tetrahydroimidazo<1,5-c>pyrimidin-5-on

: 586344-24-3
methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 24 h / Heating

2: 260 mg / DIPEA / tetrahydrofuran / 16 h / Heating

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.200204445

Reference yield:

: 1499-46-3
L-Histidine methyl ester

: 586344-24-3
methyl N-[(benzyloxy)carbonyl]-1-(2-tert-butoxy-2-oxoethyl) histidinate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / dimethylformamide / 6 h / 70 °C

2: acetonitrile / 24 h / Heating

3: 260 mg / DIPEA / tetrahydrofuran / 16 h / Heating

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.200204445