C₂₆H₂₂N₂O₂S

Base Information

• Chemical Name: C₂₆H₂₂N₂O₂S
• CAS No.: 790661-18-6
• Molecular Formula: C₂₆H₂₂N₂O₂S
• Molecular Weight: 426.539
• Mol file: 790661-18-6.mol

Synonyms:C₂₆H₂₂N₂O₂S

Chemical Property of C₂₆H₂₂N₂O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₂N₂O₂S

There total 1 articles about C₂₆H₂₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

biphenyl-4-yl-phenyl-methanone (2128-93-0) + toluene-4-sulfonic acid hydrazide (1576-35-8) → C26H22N2O2S (790661-18-6)

Guidance literature:

In methanol; Reflux;

DOI:10.1021/ol901876w

Reference yield: 79.0%

1-bromo-4-tert-butylbenzene (3972-65-4) + C26H22N2O2S (790661-18-6) → 4-((4-(tert-butyl)phenyl)(phenyl)methyl)-1,1'-biphenyl (1428338-91-3)

Guidance literature:

With [1,1′-biphenyl]-2-yldiphenylphosphane; ammonium acetate; ammonium formate; palladium diacetate; caesium carbonate; In tert-Amyl alcohol; at 90 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ol400690t

Reference yield: 67.0%

C26H22N2O2S (790661-18-6) + 3-Butyn-1-ol (927-74-2) → (E)-2-([1,1'-biphenyl]-4-yl(phenyl)methylene)tetrahydrofuran

Guidance literature:

C₂₆H₂₂N₂O₂S; 3-Butyn-1-ol; With copper(l) iodide; bathophenanthroline; tetrabutylammomium bromide; lithium tert-butoxide; In 1,4-dioxane; at 110 ℃; for 4h; Inert atmosphere;

With toluene-4-sulfonic acid; at 80 ℃; for 2h; stereoselective reaction; Inert atmosphere;

DOI:10.1016/S1872-2067(16)62565-2

upstream raw materials:

biphenyl-4-yl-phenyl-methanone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

C₂₆H₂₀

4-(1-phenylbuta-1,3-dien-1-yl)-1,1'-biphenyl

4-((4-(tert-butyl)phenyl)(phenyl)methyl)-1,1'-biphenyl

4-benzylbiphenyl