diphenylboronium dimethylbis(2-pyridylborate)

Base Information

Chemical Name:diphenylboronium dimethylbis(2-pyridylborate)
CAS No.:175605-34-2
Molecular Formula:C₂₄H₂₄B₂N₂
Molecular Weight:362.09
Hs Code.:

Synonyms:diphenylboronium dimethylbis(2-pyridylborate)

Suppliers and Price of diphenylboronium dimethylbis(2-pyridylborate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diphenylboronium dimethylbis(2-pyridylborate)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diphenylboronium dimethylbis(2-pyridylborate)

There total 1 articles about diphenylboronium dimethylbis(2-pyridylborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 175605-33-1
hydrogen dimethylbis(2-pyridyl)borate

: 5123-17-1
bromodiphenylborane

: 175605-34-2
diphenylboronium dimethylbis(2-pyridylborate)

Guidance literature:: With BuLi; In diethyl ether; hexane; byproducts: butane, LiBr; N2-atmosphere; addn. of BuLi (in hexane) to pyridylborane (in hexane/Et2O) at -78°C, stirring for 15 min, addn. of Ph2BBr (in hexane), stirring for 15 h with warming to room temp.; collection (filtration), washing (1 M aq. AcOH, water), drying in air; further crop from filtrate on evapn. and extn. into hexane; can be recrystallized (hexane/THF); elem. anal.;
DOI:10.1021/ic950775m