C₅₅H₅₇F₁₅N₄Si₂

Base Information

• Chemical Name: C₅₅H₅₇F₁₅N₄Si₂
• CAS No.: 1379604-93-9
• Molecular Formula: C₅₅H₅₇F₁₅N₄Si₂
• Molecular Weight: 1115.23
• Mol file: 1379604-93-9.mol

Synonyms:C₅₅H₅₇F₁₅N₄Si₂

Chemical Property of C₅₅H₅₇F₁₅N₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₅₅H₅₇F₁₅N₄Si₂

There total 1 articles about C₅₅H₅₇F₁₅N₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C20H26F5NOSi (1379604-82-6) + 5-(pentafluorophenyl)dipyrromethane (167482-91-9) → C55H57F15N4Si2 (1379604-93-9)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.201103034

Reference yield: 99.0%

C55H57F15N4Si2 (1379604-93-9) → C37H17F15N4 (1379605-06-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1.08333h; Inert atmosphere;

DOI:10.1002/chem.201103034

Reference yield:

C55H57F15N4Si2 (1379604-93-9) → corrorin (352430-54-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.08 h / 20 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / Inert atmosphere

With tetrabutyl ammonium fluoride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; acetonitrile;

DOI:10.1002/chem.201103034

upstream raw materials:

C₂₀H₂₆F₅NOSi

5-(pentafluorophenyl)dipyrromethane

Downstream raw materials:

C₃₇H₁₇F₁₅N₄

corrorin