C₅₀H₅₉ClN₂₄O₂₄

Base Information

Chemical Name:C₅₀H₅₉ClN₂₄O₂₄
CAS No.:620172-10-3
Molecular Formula:C₅₀H₅₉ClN₂₄O₂₄
Molecular Weight:1415.62
Hs Code.:

C<sub>50</sub>H<sub>59</sub>ClN<sub>24</sub>O<sub>24</sub>

Synonyms:C₅₀H₅₉ClN₂₄O₂₄

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Chemical Property of C₅₀H₅₉ClN₂₄O₂₄

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Technology Process of C₅₀H₅₉ClN₂₄O₂₄

There total 10 articles about C₅₀H₅₉ClN₂₄O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 620172-01-2
ethyl 2-O-benzoyl-3,4-dideoxy-3,4-diazido-6-O-chloroacetyl-1-thio-β-D-allopyranoside

: 620172-08-9
acetic acid 2-[3-acetoxy-4-(4,5-diacetoxy-3-azido-6-azidomethyl-tetrahydro-pyran-2-yloxy)-5-hydroxymethyl-tetrahydro-furan-2-yloxy]-4,6-diazido-3-(4,5-diacetoxy-3-azido-6-azidomethyl-tetrahydro-pyran-2-yloxy)-cyclohexyl ester

: 620172-10-3
C₅₀H₅₉ClN₂₄O₂₄

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1021/ol035213i

Reference yield:

: 56245-60-4,686299-00-3
ethyl 1-thio-β-D-galactopyranoside

: 620172-10-3
C₅₀H₅₉ClN₂₄O₂₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: DMAP / pyridine / 0.5 h / 60 °C

2.1: camphorsulfonic acid / acetone / 3 h / 20 °C

3.1: DMAP / pyridine / 4 h / 20 °C

4.1: 4.34 g / AcOH / tetrahydrofuran; H₂O / 5 h / 60 °C

5.1: Tf₂O; pyridine / CH₂Cl₂ / 0.25 h / 0 °C

5.2: 63 percent / NaN₃; HMPA / CH₂Cl₂; dimethylformamide / 3 h / 50 °C

6.1: HF*Py / pyridine / 5 h / 0 °C

7.1: 777 mg / DMAP; pyridine / 0.42 h

8.1: 81 percent / 4 Angstroem molecular sieves; NIS; TfOH / CH₂Cl₂ / 0.17 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; 4 A molecular sieve; camphor-10-sulfonic acid; pyridine hydrogenfluoride; acetic acid; In tetrahydrofuran; pyridine; dichloromethane; water; acetone;
DOI:10.1021/ol035213i

Reference yield:

: Benzoic acid (2S,3R,4R,5S,6S)-4,5-diazido-2-ethylsulfanyl-6-hydroxymethyl-tetrahydro-pyran-3-yl ester

: 620172-10-3
C₅₀H₅₉ClN₂₄O₂₄

Guidance literature:: Multi-step reaction with 2 steps

1: 777 mg / DMAP; pyridine / 0.42 h

2: 81 percent / 4 Angstroem molecular sieves; NIS; TfOH / CH₂Cl₂ / 0.17 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/ol035213i