[2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester

Base Information

• Chemical Name: [2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester
• CAS No.: 298690-31-0
• Molecular Formula: C₃₀H₅₀N₂O₅Si
• Molecular Weight: 546.823

Synonyms:[2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester

Chemical Property of [2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester

Chemical Property:

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Technology Process of [2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester

There total 1 articles about [2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

urethane (51-79-6) + (di-tert-butyl-oct-1-ynyl-silanyloxy)-phenyl-acetaldehyde → [2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester (298690-31-0)

Guidance literature:

With (1S)-10-camphorsulfonic acid; In benzene; at 20 ℃; for 12h;

DOI:10.1016/S0040-4039(00)00936-9

Reference yield:

[2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester (298690-31-0) → 1,1-di-tert-butyl-5-ethoxy-7-hexyl-3-phenyl-3,3a-dihydro-1H-2,6-dioxa-4-aza-1-sila-indene

Guidance literature:

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 20 ℃; for 4h;

DOI:10.1016/S0040-4039(00)00936-9

Reference yield:

[2-(di-tert-butyl-oct-1-ynyl-silanyloxy)-1-ethoxycarbonylamino-2-phenyl-ethyl]-carbamic acid ethyl ester (298690-31-0) → ((4R,5R)-2,2-Di-tert-butyl-3-heptanoyl-5-phenyl-[1,2]oxasilolan-4-yl)-carbamic acid ethyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: BF₃*OEt₂ / 1,2-dichloro-ethane / 4 h / 20 °C

2: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 20 h / 20 °C

With boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; In 1,2-dichloro-ethane; 1: Cyclization / 2: Ring cleavage;

DOI:10.1016/S0040-4039(00)00936-9

upstream raw materials:

urethane

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