3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

Base Information

Chemical Name:3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole
CAS No.:115495-60-8
Molecular Formula:C₂₄H₂₉NO₃
Molecular Weight:379.499
Hs Code.:

Synonyms:3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

Suppliers and Price of 3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

There total 1 articles about 3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 107487-01-4
(5-Pentyl-4,5-dihydro-isoxazol-3-ylmethyl)-phosphonic acid diethyl ester

: 115495-60-8
3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, THF, -78 deg C, 30 min; 2.) -78 deg C, 1 h, r.t., 4 h;
DOI:10.1246/bcsj.60.4091

Reference yield: 68.0%

: 115495-60-8
3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

: 39886-80-1,51134-90-8,72724-06-2,79080-41-4
1-(4-benzyloxy-3-methoxyphenyl)-5-hydroxydecan-3-one

Guidance literature:: With hydrogen; boric acid; Raney Ni W-2; In ethanol; dichloromethane; water; for 48h; Ambient temperature;
DOI:10.1246/bcsj.60.4091

Reference yield:

: 115495-60-8
3-[(E)-2-(4-Benzyloxy-3-methoxy-phenyl)-vinyl]-5-pentyl-4,5-dihydro-isoxazole

: 23513-14-6,72749-01-0,74027-33-1,39886-76-5,1391-73-7
(+/-)-[6]-gingerol

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / hydrogen, boric acid / Raney Ni W-2 / ethanol; CH₂Cl₂; H₂O / 48 h / Ambient temperature

2: 100 percent / hydrogen / 5 percent palladium on charcoal / methanol / 7 h / Ambient temperature

With hydrogen; boric acid; palladium on activated charcoal; Raney Ni W-2; In methanol; ethanol; dichloromethane; water;
DOI:10.1246/bcsj.60.4091