5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

Base Information

Chemical Name:5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)
CAS No.:1332509-45-1
Molecular Formula:C₉₀H₁₂₄BrN₅O₄Zn
Molecular Weight:1485.3
Hs Code.:

Synonyms:5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

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Chemical Property of 5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

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Technology Process of 5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

There total 1 articles about 5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.23%

: 1332509-44-0
[5,15-dibromo-10,20-bis(2,6-didodecoxyphenyl)porphyrinato] zinc(II)

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 1332509-45-1
5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 40 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c1cc12764k

Reference yield: 96.8%

: 1332509-45-1
5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

: 89343-06-6
tris-iso-propylsilyl acetylene

: C₁₀₁H₁₄₅N₅O₄SiZn

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 60 ℃; for 6h; Inert atmosphere; Glovebox;
DOI:10.1039/c4ta06589a

Reference yield: 73.0%

: 206768-21-0
5-ethynyl-thiophene-2-carbaldehyde

: 1332509-45-1
5-bromo-15-(4-N,N-dimethylamino-phenyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato zinc(II)

: C₉₇H₁₂₇N₅O₅SZn

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 45 ℃; for 14h; Inert atmosphere;
DOI:10.1039/c3ta11870c