(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

Base Information

Chemical Name:(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate
CAS No.:1589529-11-2
Molecular Formula:C₁₄H₁₆O₃
Molecular Weight:232.279
Hs Code.:

Synonyms:(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

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Chemical Property of (S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

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Technology Process of (S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

There total 4 articles about (S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1589529-07-6
(S)-3-hydroxy-4-(tosyloxy)butyl 2-allylbenzoate

: 1589529-11-2
(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃;
DOI:10.1021/ja500726e

Reference yield:

: 1589529-06-5
(S)-3,4-dihydroxybutyl 2-allylbenzoate

: 1589529-11-2
(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; di(n-butyl)tin oxide / dichloromethane / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

With di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane;
DOI:10.1021/ja500726e

Reference yield:

: 66657-85-0
2-allylbenzoyl chloride

: 1589529-11-2
(S)-2-(oxiran-2-yl)ethyl 2-allylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; pyridine / dichloromethane / 0.5 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane; water / 1 h / 0 °C

3: triethylamine; di(n-butyl)tin oxide / dichloromethane / 20 °C

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

With pyridine; dmap; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1021/ja500726e