N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

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Chemical Name:N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester
CAS No.:1192142-96-3
Molecular Formula:C₁₀₂H₁₀₄N₂O₂₁
Molecular Weight:1693.95
Hs Code.:

N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

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Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

There total 1 articles about N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1192142-94-1
N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

: 1192142-96-3
N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at -10 ℃; for 0.5h;
DOI:10.1016/j.tet.2009.07.080

Reference yield: 97.0%

: 1192142-96-3
N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

: N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-3-O-sulfo-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

Guidance literature:: With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.080