2-phenyl-1,3,2-dithiaphospholane

Base Information

• Chemical Name: 2-phenyl-1,3,2-dithiaphospholane
• CAS No.: 4669-54-9
• Molecular Formula: C8H9PS2
• Molecular Weight: 200.2608
• Mol file: 4669-54-9.mol

Synonyms:

Chemical Property of 2-phenyl-1,3,2-dithiaphospholane

Chemical Property:

• Vapor Pressure: 0.000918mmHg at 25°C
• Boiling Point: 313.4°Cat760mmHg
• Flash Point: 143.3°C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-phenyl-1,3,2-dithiaphospholane

There total 2 articles about 2-phenyl-1,3,2-dithiaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloro-1,3,2-dithiaphospholane (4669-51-6) → 2-phenyl-1,3-dithia-2-phosphacyclopentane (4669-54-9)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1021/jo00105a007

Reference yield:

→ 2-phenyl-1,3-dithia-2-phosphacyclopentane (4669-54-9)

Guidance literature:

Verb. I, Phenyldichlorphosphin;

DOI:10.1002/zaac.19673550310

Reference yield: 82.0%

2-phenyl-1,3-dithia-2-phosphacyclopentane (4669-54-9) → ethylene phenylphosphonotrithioate (29021-62-3)

Guidance literature:

With sulfur; In benzene;

DOI:10.1021/jo00105a007

upstream raw materials:

2-Chloro-1,3,2-dithiaphospholane

Downstream raw materials:

ethylene phenylphosphonotrithioate

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