C₃₃H₃₃NO₇

Base Information

Chemical Name:C₃₃H₃₃NO₇
CAS No.:1395875-07-6
Molecular Formula:C₃₃H₃₃NO₇
Molecular Weight:555.628
Hs Code.:

C<sub>33</sub>H<sub>33</sub>NO<sub>7</sub>

Synonyms:C₃₃H₃₃NO₇

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Chemical Property of C₃₃H₃₃NO₇

Chemical Property:

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Technology Process of C₃₃H₃₃NO₇

There total 5 articles about C₃₃H₃₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1395872-59-9
C₃₁H₃₃NO₇

: 108-24-7
acetic anhydride

: 1395875-07-6
C₃₃H₃₃NO₇

Guidance literature:: With sodium acetate; In toluene; for 3h; Reflux;

Reference yield:

: 25118-59-6
4-bromo-3-chlorobenzoic acid

: 1395875-07-6
C₃₃H₃₃NO₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 25 °C

1.2: 4 h / -50 - 25 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; ethanol; water / 3 h / Inert atmosphere; Reflux

3.1: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 3 h / Reflux

4.1: potassium tert-butylate / tetrahydrofuran / 1 h / 55 °C

5.1: sodium acetate / toluene / 3 h / Reflux

With oxalyl dichloride; tri-tert-butyl phosphine; potassium tert-butylate; sodium acetate; sodium carbonate; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; N,N-dimethyl-formamide; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; toluene;

Reference yield:

: 1196395-67-1
(4-bromo-3-chlorophenyl)-phenylmethanone

: 1395875-07-6
C₃₃H₃₃NO₇

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; ethanol; water / 3 h / Inert atmosphere; Reflux

2: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 3 h / Reflux

3: potassium tert-butylate / tetrahydrofuran / 1 h / 55 °C

4: sodium acetate / toluene / 3 h / Reflux

With tri-tert-butyl phosphine; potassium tert-butylate; sodium acetate; sodium carbonate; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; toluene;