(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

Base Information

Chemical Name:(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide
CAS No.:1335214-42-0
Molecular Formula:C₂₉H₃₇NO₅
Molecular Weight:479.616
Hs Code.:

Synonyms:(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

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Chemical Property of (+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

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Technology Process of (+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

There total 6 articles about (+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 193749-08-5
C₁₅H₁₉NO₄

: (+)-(1R,2S)-trans-phenylcyclohexanol vinyl ether

: 1335214-42-0
(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -94 ℃;
DOI:10.1039/c3ob41646a

Reference yield:

: 193749-08-5
C₁₅H₁₉NO₄

: (+)-(1R,2S)-trans-phenylcyclohexanol vinyl ether

: 1335214-42-0
(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

: 4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-((-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -94 ℃; Overall yield = 75 percent;
DOI:10.3390/molecules25163613

Reference yield:

: 193749-08-5
C₁₅H₁₉NO₄

: (+)-(1R,2S)-trans-phenylcyclohexanol vinyl ether

: 1335214-42-0
(+)-(4S,6S)-4-(3-(cyclopentyloxy)-4-methoxyphenyl)-3-methyl-6-(((1S,2R)-2-phenylcyclohexyl)oxy)-5,6-dihydro-4H-1,2-oxazine-2-oxide

: (4R,6R,7S,8R)-4-[3-(cyclopentyloxy)-4-(methyloxy)phenyl]-3-methyl-6-[(2-phenylcyclohexyl)oxy]-5,6-dihydro-4H-1,2-oxazine 2-oxide

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -90 ℃; for 0.166667h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo201331h