1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide

Base Information

Chemical Name:1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide
CAS No.:1235456-21-9
Molecular Formula:C₃₈H₅₈N₂OSi₂
Molecular Weight:615.062
Hs Code.:

Synonyms:1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide

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Chemical Property of 1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide

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Technology Process of 1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide

There total 2 articles about 1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 53906-85-7
3,5-dimethyl-4-iodonitrobenzene

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1235456-20-8
3,5-dimethyl-4-(triisopropylsilylethynyl)nitrobenzene

: 1235456-21-9
1,2-bis(3,5-dimethyl-4-((triisopropylsilyl)ethynyl)phenyl)diazene oxide

Guidance literature:: 3,5-dimethyl-4-iodonitrobenzene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; for 0.333333h; Inert atmosphere; Sonication;

tris-iso-propylsilyl acetylene; In tetrahydrofuran; at 45 - 50 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ja103235g