Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

Base Information

Chemical Name:Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate
CAS No.:82749-82-4
Molecular Formula:C₁₇H₁₅N₂O₇S₂*K
Molecular Weight:462.546
Hs Code.:

Synonyms:Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

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Chemical Property of Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

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Technology Process of Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

There total 6 articles about Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 82749-80-2
phenyl N-furfuryl-4-phenoxy-5-sulfamoylothanilate

: 82749-82-4
Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

Guidance literature:: With potassium hydroxide; for 6h; Heating;
DOI:10.1021/jm00362a017

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 82749-82-4
Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / propan-2-ol / 10 h / Heating

2: 76 percent / 2N aq. KOH / 6 h / Heating

With potassium hydroxide; In isopropyl alcohol;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 82749-82-4
Potassium; 2-[(furan-2-ylmethyl)-amino]-4-phenoxy-5-sulfamoyl-benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 50 percent / butan-2-one / 6 h / Heating

3: 52 percent / propan-2-ol / 10 h / Heating

4: 76 percent / 2N aq. KOH / 6 h / Heating

With potassium hydroxide; ammonia; In isopropyl alcohol; butanone;
DOI:10.1021/jm00362a017