C₂₂H₂₃F₄NO₄

Base Information

Chemical Name:C₂₂H₂₃F₄NO₄
CAS No.:1078725-44-6
Molecular Formula:C₂₂H₂₃F₄NO₄
Molecular Weight:441.423
Hs Code.:

C<sub>22</sub>H<sub>23</sub>F<sub>4</sub>NO<sub>4</sub>

Synonyms:C₂₂H₂₃F₄NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₃F₄NO₄

Chemical Property:

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Technology Process of C₂₂H₂₃F₄NO₄

There total 7 articles about C₂₂H₂₃F₄NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1078725-43-5
C₂₃H₂₅F₄NO₄

: 1078725-44-6
C₂₂H₂₃F₄NO₄

Guidance literature:: With boron tribromide; In dichloromethane; at -78 ℃;
DOI:10.3987/COM-08-11407

Reference yield:

: C₂₂H₂₄FNO₅

: 1078725-44-6
C₂₂H₂₃F₄NO₄

Guidance literature:: Multi-step reaction with 6 steps

1: triethylsilane / dichloromethane / 20 °C

2: titanium(IV) tetraethanolate / 80 °C

3: titanium tetrachloride / dichloromethane / -78 - 20 °C

4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C

6: boron tribromide / dichloromethane / -78 °C

With triethylsilane; titanium(IV) tetraethanolate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; boron tribromide; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; water; tert-butyl alcohol; 4: Kraus oxidation;
DOI:10.3987/COM-08-11407

Reference yield:

: 331-64-6
2-fluoro-4-methoxy-benzaldehyde

: 1078725-44-6
C₂₂H₂₃F₄NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C

2: triethylsilane / dichloromethane / 20 °C

3: titanium(IV) tetraethanolate / 80 °C

4: titanium tetrachloride / dichloromethane / -78 - 20 °C

5: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C

7: boron tribromide / dichloromethane / -78 °C

With triethylsilane; titanium(IV) tetraethanolate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-n-butylboryl trifluoromethanesulfonate; boron tribromide; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; water; tert-butyl alcohol; 1: Evans's asymmetric aldol condensation / 5: Kraus oxidation;
DOI:10.3987/COM-08-11407