4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Base Information

Chemical Name:4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde
CAS No.:1397706-66-9
Molecular Formula:C₃₁H₂₈O₅
Molecular Weight:480.56
Hs Code.:

Synonyms:4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Suppliers and Price of 4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

There total 3 articles about 4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 93727-83-4
4,4'-(5-hydroxypentane-2,2-diyl)diphenol

: 459-57-4
4-fluorobenzaldehyde

: 1397706-66-9
4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Guidance literature:: 4,4'-(5-hydroxypentane-2,2-diyl)diphenol; With potassium carbonate; In acetone; for 0.166667h;

4-fluorobenzaldehyde; In acetone; for 8h; Reflux;
DOI:10.1016/j.reactfunctpolym.2012.06.020

Reference yield:

: 126-00-1
4,4-bis(4-hydroxyphenyl)valeric acid

: 1397706-66-9
4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 8 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / Reflux

3.1: potassium carbonate / acetone / 0.17 h

3.2: 8 h / Reflux

With lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; In tetrahydrofuran; acetone; 1.1: |Fischer-Speier Esterification;
DOI:10.1016/j.reactfunctpolym.2012.06.020

Reference yield:

: 7297-85-0
4-hydroxy-γ-(4-hydroxyphenyl)-γ-methyl-benzenebutanoic acid methyl ester

: 1397706-66-9
4,4'-(4,4'-(5-hydroxypentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)dibenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / Reflux

2.1: potassium carbonate / acetone / 0.17 h

2.2: 8 h / Reflux

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.reactfunctpolym.2012.06.020