Technology Process of C17H16F3NO2S2
There total 6 articles about C17H16F3NO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; ethyl crotonate; nickel dichloride; zinc;
In
methanol;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ol303366u
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: potassium carbonate / methanol / 20 °C / Inert atmosphere
3.1: zinc; nickel dichloride; pyridine; ethyl crotonate / methanol / 20 °C / Inert atmosphere
With
pyridine; ethyl crotonate; potassium carbonate; caesium carbonate; nickel dichloride; zinc;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol303366u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / methanol / 20 °C / Inert atmosphere
2: zinc; nickel dichloride; pyridine; ethyl crotonate / methanol / 20 °C / Inert atmosphere
With
pyridine; ethyl crotonate; potassium carbonate; nickel dichloride; zinc;
In
methanol;
DOI:10.1021/ol303366u