N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester

Base Information

• Chemical Name: N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester
• CAS No.: 1033470-93-7
• Molecular Formula: C₂₂H₂₅NO₅
• Molecular Weight: 383.444
• Mol file: 1033470-93-7.mol

Synonyms:N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester

Chemical Property of N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester

There total 1 articles about N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N-[(phenylmethoxy)carbonyl]-L-tyrosine (16679-94-0) + allyl bromide (106-95-6) → N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester (1033470-93-7)

Guidance literature:

With potassium carbonate; In acetone; for 4h; Heating;

DOI:10.1016/j.tetlet.2008.03.099

Reference yield: 22.0%

N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester (1033470-93-7) → N-benzyloxycarbonyl-O'-(2-oxoethyl)-L-tyrosine ethyl ester (1033471-05-4)

Guidance literature:

N-benzyloxycarbonyl-O'-(prop-2-enyl)-L-tyrosine ethyl ester; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at 20 ℃; Further stages.;

DOI:10.1016/j.tetlet.2008.03.099

upstream raw materials:

N-[(phenylmethoxy)carbonyl]-L-tyrosine

allyl bromide

Downstream raw materials:

N-benzyloxycarbonyl-O'-(2-oxoethyl)-L-tyrosine ethyl ester