Technology Process of C24H34O5S
There total 9 articles about C24H34O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; hydrogen;
Lindlar's catalyst;
In
benzene;
under 760.051 Torr;
Title compound not separated from byproducts.;
DOI:10.1002/anie.200701515
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-BuLi / diethyl ether / -78 °C
1.2: MgBr2*OEt2 / diethyl ether / -78 - 0 °C
1.3: THF / diethyl ether / 20 °C
2.1: 4-dimethylaminopyridine; pyridine / CH2Cl2
3.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH3*SMe2 / tetrahydrofuran / 0 °C
4.1: H2; pyridine / Pd/CaCO3/Pb / benzene / 760.05 Torr
With
pyridine; dmap; n-butyllithium; dimethylsulfide borane complex; hydrogen; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole;
Lindlar's catalyst;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
3.1: Corey-Bakshi-Shibata reduction;
DOI:10.1002/anie.200701515
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH3*SMe2 / tetrahydrofuran / 0 °C
2: H2; pyridine / Pd/CaCO3/Pb / benzene / 760.05 Torr
With
pyridine; dimethylsulfide borane complex; hydrogen; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole;
Lindlar's catalyst;
In
tetrahydrofuran; benzene;
1: Corey-Bakshi-Shibata reduction;
DOI:10.1002/anie.200701515
