[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

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Chemical Name:[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)
CAS No.:1351986-29-2
Molecular Formula:C₅₂H₅₈Br₂N₄NiO₄
Molecular Weight:1021.55
Hs Code.:

Synonyms:[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

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Chemical Property of [5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

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Technology Process of [5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

There total 1 articles about [5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 5,15-dibromo-10,20-bis[3,5-bis(3-methylbutoxy)phenyl]porphyrin

: 1351986-29-2
[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

Guidance literature:: With nickel(II) acetate tetrahydrate; In N,N-dimethyl-formamide; at 140 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1021/ol202973z

Reference yield: 88.0%

: 1351986-29-2
[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

: 1351986-30-5
[5,15-diazido-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 40 ℃; for 0.166667h; Inert atmosphere; Darkness;
DOI:10.1021/ol202973z

Reference yield:

: 1351986-29-2
[5,15-dibromo-10,20-bis(3,5-bis(3-methylbutoxy)phenyl)porphyrinato]nickel(II)

: C₅₂H₆₂N₆NiO₄

Guidance literature:: With sodium azide; potassium carbonate; sodium L-ascorbate; In N,N-dimethyl-formamide; at 40 - 90 ℃; for 3.5h; Inert atmosphere; Darkness;
DOI:10.1021/acs.joc.6b02159