(S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

Base Information

Chemical Name:(S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate
CAS No.:1586007-59-1
Molecular Formula:C₂₈H₃₂N₂O₂
Molecular Weight:428.574
Hs Code.:

Synonyms:(S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

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Chemical Property of (S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

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Technology Process of (S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

There total 1 articles about (S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21040-45-9
Cinnamyl acetate

: methyl 2-(4-dimethylaminophenylimino)-2-phenylacetate

: 925-90-6
ethylmagnesium bromide

: 1586007-59-1
(S,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

: (R,E)-methyl 2-((4-(dimethylamino)phenyl)(ethyl)amino)-2,5-diphenylpent-4-enoate

Guidance literature:: methyl 2-(4-dimethylaminophenylimino)-2-phenylacetate; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;

Cinnamyl acetate; With bis(η3-allyl-μ-chloropalladium(II)); (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Overall yield = 74 %; Overall yield = 62 mg; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol500506t