{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester
CAS No.:852873-25-7
Molecular Formula:C₄₁H₅₂N₄O₁₁
Molecular Weight:776.884
Hs Code.:

{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

Synonyms:{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

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Chemical Property of {(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

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Technology Process of {(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

There total 6 articles about {(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R,3R,4R,5S,6R)-6-Azidomethyl-3-tert-butoxycarbonylamino-4,5-dihydroxy-tetrahydro-pyran-2-carboxylic acid

: 852873-25-7
{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / P₂O₅ / tetrahydrofuran

2: NaOH / methanol

3: H₂ / Pd/C / methanol

4: Na₂CO₃ / H₂O; acetone

5: 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium*PF₆; 1-hydroxybenzotriazole; iPr₂NEt / dimethylformamide; CHCl₃

With sodium hydroxide; hydrogen; phosphorus pentoxide; sodium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/anie.200462595

Reference yield:

: 852873-21-3
(2R,3R,4R,5R,6R)-6-Azidomethyl-3-tert-butoxycarbonylamino-4,5-bis-methoxymethoxy-tetrahydro-pyran-2-carboxylic acid methoxymethyl ester

: 852873-25-7
{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH / methanol

2: H₂ / Pd/C / methanol

3: Na₂CO₃ / H₂O; acetone

4: 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium*PF₆; 1-hydroxybenzotriazole; iPr₂NEt / dimethylformamide; CHCl₃

With sodium hydroxide; hydrogen; sodium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/anie.200462595

Reference yield:

: (2R,3R,4R,5R,6R)-6-Azidomethyl-3-tert-butoxycarbonylamino-4,5-bis-methoxymethoxy-tetrahydro-pyran-2-carboxylic acid

: 852873-25-7
{(2R,3R,4R,5R,6R)-2-(2-Benzylcarbamoyl-ethylcarbamoyl)-6-[(9H-fluoren-9-ylmethoxycarbonylamino)-methyl]-4,5-bis-methoxymethoxy-tetrahydro-pyran-3-yl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol

2: Na₂CO₃ / H₂O; acetone

3: 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium*PF₆; 1-hydroxybenzotriazole; iPr₂NEt / dimethylformamide; CHCl₃

With hydrogen; sodium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/anie.200462595