(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

Base Information

Chemical Name:(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone
CAS No.:1463609-38-2
Molecular Formula:C₂₂H₂₀ClN₃O
Molecular Weight:377.873
Hs Code.:

Synonyms:(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

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Chemical Property of (4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

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Technology Process of (4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

There total 4 articles about (4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₀ClNO₃

: 1463609-38-2
(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

Guidance literature:: With hydrazine hydrate; acetic acid; In ethanol; for 4h; Reflux;
DOI:10.3390/molecules18078147

Reference yield:

: 5274-99-7
1-benzoylisonipecotic acid

: 1463609-38-2
(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 14 h / 40 °C

2: sodium hydride / mineral oil / 3.5 h / Reflux

3: hydrazine hydrate; acetic acid / ethanol / 4 h / Reflux

With dmap; sodium hydride; hydrazine hydrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; mineral oil;
DOI:10.3390/molecules18078147

Reference yield:

: 1463609-37-1
phenyl 1-benzoylpiperidine-4-carboxylate

: 1463609-38-2
(4-(6-chloro-1,4-dihydroindeno[1,2-c]pyrazol-3-yl)piperidin-1-yl)(phenyl)metanone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil / 3.5 h / Reflux

2: hydrazine hydrate; acetic acid / ethanol / 4 h / Reflux

With sodium hydride; hydrazine hydrate; acetic acid; In ethanol; mineral oil;
DOI:10.3390/molecules18078147