4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

Base Information

Chemical Name:4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester
CAS No.:66642-78-2
Molecular Formula:C₂₄H₂₈O₁₂
Molecular Weight:508.479
Hs Code.:

4-(tetra-<i>O</i>-acetyl-β-D-glucopyranosyloxy)-<i>trans</i>-cinnamic acid methyl ester

Synonyms:4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

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Chemical Property of 4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

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Technology Process of 4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

There total 4 articles about 4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 669763-44-4
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(4-iodophenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 66642-78-2
4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In acetonitrile; at 70 ℃;
DOI:10.1055/s-2003-43376

Reference yield:

: 4468-72-8
phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 66642-78-2
4-(tetra-O-acetyl-β-D-glucopyranosyloxy)-trans-cinnamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / ceric ammonium nitrate; n-Bu₄NI / acetonitrile / 24 h / 70 °C

2: 89 percent / P(o-tol)3; Et₃N / Pd(OAc)2 / acetonitrile / 70 °C

With ammonium cerium(IV) nitrate; tetra-(n-butyl)ammonium iodide; triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In acetonitrile; 2: Heck reaction;
DOI:10.1055/s-2003-43376