N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

Base Information

Chemical Name:N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester
CAS No.:134363-60-3
Molecular Formula:C₂₁H₃₂N₂O₆
Molecular Weight:408.495
Hs Code.:

Synonyms:N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

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Chemical Property of N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

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Technology Process of N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

There total 3 articles about N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7479-01-8
O-methyl-L-tyrosine methyl ester hydrochloride

: 134363-60-3
N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / N-methylmorpholine, DMAP, DMF / CH₂Cl₂ / 36 h / Ambient temperature

2: 87 percent / H₂ / 10percent Pd/C / ethyl acetate / 2.5 h

3: 1.97 g / CH₂Cl₂ / 16 h / Ambient temperature

With 4-methyl-morpholine; dmap; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00056a005

Reference yield:

: 134363-80-7
N-<3-<(benzyloxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

: 134363-60-3
N-<3-<(tert-butoxycarbonyl)amino>-3,3-dimethylpropionyl>-O-methyltyrosine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / H₂ / 10percent Pd/C / ethyl acetate / 2.5 h

2: 1.97 g / CH₂Cl₂ / 16 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00056a005