5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

Base Information

Chemical Name:5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide
CAS No.:85945-69-3
Molecular Formula:C₂₂H₂₉N₃O₃S₂
Molecular Weight:447.623
Hs Code.:

Synonyms:5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

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Chemical Property of 5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

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Technology Process of 5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

There total 5 articles about 5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 85945-58-0
2-(4-Cyano-benzenesulfonylamino)-5-phenyl-pentanoic acid butylamide

: 85945-69-3
5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

Guidance literature:: With hydrogen sulfide; In pyridine; triethylamine; Ambient temperature;

Reference yield:

: 34993-02-7,2046-19-7
2-(R)-amino-5-phenylpentanoic acid

: 85945-69-3
5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / 1) 1 M NaOH; 2) HCl/H₂O / diethyl ether / 20 h / Ambient temperature

2: SOCl₂ / 1 h / Heating

3: 74 percent / benzene / 1.5 h

4: 89 percent / H₂S / pyridine; triethylamine / Ambient temperature

With hydrogenchloride; sodium hydroxide; thionyl chloride; hydrogen sulfide; water; In pyridine; diethyl ether; triethylamine; benzene;

Reference yield:

: 85945-47-7
2-(4-Cyano-benzenesulfonylamino)-5-phenyl-pentanoyl chloride

: 85945-69-3
5-Phenyl-2-(4-thiocarbamoyl-benzenesulfonylamino)-pentanoic acid butylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / benzene / 1.5 h

2: 89 percent / H₂S / pyridine; triethylamine / Ambient temperature

With hydrogen sulfide; In pyridine; triethylamine; benzene;