Technology Process of C23H32O4
There total 10 articles about C23H32O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 50 percent / KH / tetrahydrofuran / 0 °C
2: 1.) NaH, 2.) DIBAL / 1.) THF, 0 deg C
3: 85 percent / CH3CH2COOH / xylene / Heating
5: 1.) NH2OH*HCl, NaOAc/AcOH, 2.) (CF3CO2)2O
6: 1.) Bu3SnH, AIBN, 2.) silica gel / 1.) benzene, reflux, 2.) CH2Cl2
7: 88 percent / DIBAL
8: 1.) PhOCSCl, 2.) Bu3SnH
9: 94 percent / Et2Zn / toluene / 60 °C
10: 60 percent / DIBAL
With
2,2'-azobis(isobutyronitrile); (CF3CO2)2O; hydroxylamine hydrochloride; diethylzinc; tri-n-butyl-tin hydride; sodium acetate; silica gel; potassium hydride; sodium hydride; diisobutylaluminium hydride; acetic acid; propionic acid; phenylcarbonochloridothioate;
In
tetrahydrofuran; toluene; xylene;
DOI:10.1021/jo00297a012
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 1.) NaH, 2.) DIBAL / 1.) THF, 0 deg C
2: 85 percent / CH3CH2COOH / xylene / Heating
4: 1.) NH2OH*HCl, NaOAc/AcOH, 2.) (CF3CO2)2O
5: 1.) Bu3SnH, AIBN, 2.) silica gel / 1.) benzene, reflux, 2.) CH2Cl2
6: 88 percent / DIBAL
7: 1.) PhOCSCl, 2.) Bu3SnH
8: 94 percent / Et2Zn / toluene / 60 °C
9: 60 percent / DIBAL
With
2,2'-azobis(isobutyronitrile); (CF3CO2)2O; hydroxylamine hydrochloride; diethylzinc; tri-n-butyl-tin hydride; sodium acetate; silica gel; sodium hydride; diisobutylaluminium hydride; acetic acid; propionic acid; phenylcarbonochloridothioate;
In
toluene; xylene;
DOI:10.1021/jo00297a012
