N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

Base Information

Chemical Name:N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea
CAS No.:108967-47-1
Molecular Formula:C₄₉H₄₈N₂O₁₈S
Molecular Weight:984.989
Hs Code.:

Synonyms:N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

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Chemical Property of N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

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Technology Process of N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

There total 7 articles about N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1228754-22-0
C₂₁H₂₄N₄O₉S

: 33639-91-7,41093-31-6,108967-44-8,115969-98-7
(2R,3R,4S,5S,6R)-2-amino-6-((benzoyloxy)methyl)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

: 108967-47-1
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1055/s-0029-1219393

Reference yield: 5.0%

: 14152-97-7
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate

: 108967-43-7
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosylamine hydrobromide

: 108967-47-1
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

: 109062-65-9
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl)thiourea

Guidance literature:: With pyridine; for 48h;
DOI:10.1016/S0008-6215(00)90042-9

Reference yield:

: 22435-64-9
2,3,4,6-tetra-O-acetyl-N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranosylamine

: 108967-47-1
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-N'-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / bromine / CHCl₃; H₂O / 48 h / Ambient temperature

2: 54 percent / calcium carbonate / CHCl₃; H₂O / 48 h

3: 59 percent / pyridine / 48 h

With pyridine; bromine; calcium carbonate; In chloroform; water;
DOI:10.1016/S0008-6215(00)90042-9