[W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄

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Chemical Name:[W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄
CAS No.:108214-99-9
Molecular Formula:C₃₉H₃₀NO₄P₂W*ClO₄
Molecular Weight:921.92
Hs Code.:

[W(CO)3(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)2]<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[W(CO)3(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)2]ClO<sub>4</sub>

Synonyms:[W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄

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Chemical Property of [W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄

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Technology Process of [W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄

There total 1 articles about [W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 540-80-7
tert.-butylnitrite

: 16743-03-6,38800-77-0,68738-00-1
trans-triphenylphosphane tetracarbonyltungsten

: 108214-99-9
[W(CO)3(NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[W(CO)3(NO)(P(C₆H₅)3)2]ClO₄

Guidance literature:: With perchloric acid; In ethanol; dichloromethane; water; byproducts: CO; under N2, tungsten complex suspended in CH2Cl2 and vigorously stirred at room temp., addn. of t-BuONO and 70%HClO4 (nitrosylating agent) and enough MeOH to obtain one liquid phase, (vigorously evoln. of CO), soln. stirred until gas evoln. was minimal; filtered, addn. of benzene to filtrate, crystn., filtered, washed (benzene, ethanol, pentane), elem. anal.;