[1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate

Base Information

• Chemical Name: [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate
• CAS No.: 1443532-79-3
• Molecular Formula: C₂₆H₃₀FO₃PSSe
• Molecular Weight: 551.521
• Mol file: 1443532-79-3.mol

Synonyms:[1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate

Chemical Property of [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate

There total 1 articles about [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-fluoro-4-(vinyloxy)benzene (351-93-9) + bis[2-(4-methoxyphenyl)ethyl]phosphine sulfide (1354722-40-9) → [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinothioselenoate (1443532-78-2) + [1-(4-fluorophenoxy)ethyl] bis(4-methoxyphenethyl)phosphinoselenothioate (1443532-79-3)

Guidance literature:

With selenium; In 1,4-dioxane; at 100 ℃; for 0.666667h; Overall yield = 91 %; Overall yield = 502 mg; Mechanism; Inert atmosphere;

DOI:10.1016/j.tet.2013.05.038

upstream raw materials:

1-fluoro-4-(vinyloxy)benzene

bis[2-(4-methoxyphenyl)ethyl]phosphine sulfide