methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Base Information

• Chemical Name: methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate
• CAS No.: 1209013-06-8
• Molecular Formula: C₂₄H₃₁ClN₂O₁₀S
• Molecular Weight: 575.037

Synonyms:methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property of methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property:

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Technology Process of methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

There total 1 articles about methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methyl (methyl 5-tert-butyloxycarbonylamino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-tride-oxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-05-7) → methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-06-8)

Guidance literature:

With chloro-trimethyl-silane; phenol; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm901517k

Reference yield: 75.0%

methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-06-8) + cyclopropanecarboxylic acid chloride (4023-34-1) → methyl (methyl 5-cyclopropylamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-07-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1021/jm901517k

Reference yield: 39.0%

methyl (methyl 5-amino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-06-8) + Cyclobutanecarbonyl chloride (5006-22-4) → methyl (methyl 5-cyclobutylamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209013-08-0)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm901517k

upstream raw materials:

methyl (methyl 5-tert-butyloxycarbonylamino-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-tride-oxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Downstream raw materials:

methyl (methyl 5-cyclopropylamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

methyl (methyl 5-cyclobutylamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

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