tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

Base Information

Chemical Name:tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate
CAS No.:1201687-13-9
Molecular Formula:C₁₇H₂₂ClN₇O₃
Molecular Weight:407.86
Hs Code.:

Synonyms:tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

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Chemical Property of tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

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Technology Process of tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

There total 1 articles about tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1201687-12-8
1-tert-butyl 3-ethyl (3S)-pyrazolidine-1,3-dicarboxylate

: 5-chloro-2-tetrazol-1-yl-benzylamine hydrochloride

: 1201687-13-9
tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

Guidance literature:: 1-tert-butyl 3-ethyl (3S)-pyrazolidine-1,3-dicarboxylate; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h;

5-chloro-2-tetrazol-1-yl-benzylamine hydrochloride; With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield: 59.0%

: 1201687-19-5
(R)-2-phenyl-2-(trimethylsilyloxy)acetyl chloride

: 1201687-13-9
tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate

: 1201686-93-2
(3S)-N-[5-chloro-2-(1H-tetrazol-1-yl)benzyl]-2-[(2R)-2-hydroxy-2-phenylacetyl]pyrazolidine-3-carboxamide

Guidance literature:: (R)-2-phenyl-2-(trimethylsilyloxy)acetyl chloride; tert-butyl (3S)-3-{[5-chloro-2-(1H-tetrazol-1-yl)benzyl]carbamoyl}pyrazolidine-1-carboxylate; With pyridine; In dichloromethane; at 20 ℃;

With trifluoroacetic acid; In dichloromethane; for 1h;