N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

Base Information

Chemical Name:N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride
CAS No.:1381767-20-9
Molecular Formula:C₁₃H₁₆N₂O₂S*ClH
Molecular Weight:300.809
Hs Code.:

Synonyms:N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

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Chemical Property of N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

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Technology Process of N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

There total 7 articles about N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₄N₂O₂S

: 1381767-20-9
N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

Guidance literature:: C₁₃H₁₄N₂O₂S; With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.166667h;

With hydrogenchloride; In ethyl acetate;
DOI:10.1016/j.bmc.2012.04.014

Reference yield:

: 881673-35-4
1-(methylsulfonyl)-5-phenyl-1H-pyrrole-3-carbaldehyde

: 1381767-20-9
N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0.25 h / 20 °C

2: sodium tetrahydroborate / methanol / 0.17 h / 20 °C

With sodium tetrahydroborate; In methanol;
DOI:10.1016/j.bmc.2012.04.014

Reference yield:

: 881673-34-3
[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanol

: 1381767-20-9
N-methyl-1-[1-(methylsulfonyl)-5-phenyl-1H-pyrrol-3-yl]methanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / acetonitrile / 1 h / 20 °C / Molecular sieve

2: methanol / 0.25 h / 20 °C

3: sodium tetrahydroborate / methanol / 0.17 h / 20 °C

With sodium tetrahydroborate; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In methanol; acetonitrile;
DOI:10.1016/j.bmc.2012.04.014