l-menthyl (+/-) 2-azidopropionate

Base Information

Chemical Name:l-menthyl (+/-) 2-azidopropionate
CAS No.:1188421-45-5
Molecular Formula:C₁₃H₂₃N₃O₂
Molecular Weight:253.345
Hs Code.:

Synonyms:l-menthyl (+/-) 2-azidopropionate

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Chemical Property of l-menthyl (+/-) 2-azidopropionate

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Technology Process of l-menthyl (+/-) 2-azidopropionate

There total 1 articles about l-menthyl (+/-) 2-azidopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 199186-96-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-bromopropanoate

: 1188421-45-5
l-menthyl (+/-) 2-azidopropionate

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 75 ℃; for 4h;
DOI:10.1021/ol901637w

Reference yield: 48.0%

: 1188421-45-5
l-menthyl (+/-) 2-azidopropionate

: 1188421-46-6
(-)-1H-pyrrole-2,5-dicarboxylic acid di-l-menthyl ester

: 951-98-4
2-Oxo-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: l-menthyl (+/-) 2-azidopropionate; With titanium tetrachloride; In dichloromethane; at -96 ℃; for 0.5h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -96 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In dichloromethane;
DOI:10.1021/ol901637w