(-)-epi-dexoxadrol hydrochloride

Base Information

Chemical Name:(-)-epi-dexoxadrol hydrochloride
CAS No.:104972-89-6
Molecular Formula:C₂₀H₂₃NO₂*ClH
Molecular Weight:345.869
Hs Code.:

Synonyms:(-)-epi-dexoxadrol hydrochloride

Suppliers and Price of (-)-epi-dexoxadrol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-epi-dexoxadrol hydrochloride

Chemical Property:

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Technology Process of (-)-epi-dexoxadrol hydrochloride

There total 4 articles about (-)-epi-dexoxadrol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117178-67-3
β-(-)-dioxadrol

: 104972-89-6
(-)-epi-dexoxadrol hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate;
DOI:10.1016/j.tet.2013.10.082

Reference yield:

: 1514644-66-6
(S)-benzyl-2-vinylpiperidine-1-carboxylate

: 104972-89-6
(-)-epi-dexoxadrol hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: AD-mix α; AD-mix β / tert-butyl alcohol; water / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C / 1900.13 Torr

3: toluene-4-sulfonic acid / isopropyl alcohol / 1 h / Reflux

4: hydrogenchloride / ethyl acetate

With hydrogenchloride; palladium 10% on activated carbon; AD-mix α; AD-mix β; hydrogen; toluene-4-sulfonic acid; In ethanol; water; ethyl acetate; isopropyl alcohol; tert-butyl alcohol; 1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tet.2013.10.082

Reference yield:

: 1514644-79-1
benzyl (2S)-2-[(1R)-1,2-dihydroxyethyl]piperidine-1-carboxylate

: 104972-89-6
(-)-epi-dexoxadrol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C / 1900.13 Torr

2: toluene-4-sulfonic acid / isopropyl alcohol / 1 h / Reflux

3: hydrogenchloride / ethyl acetate

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; In ethanol; ethyl acetate; isopropyl alcohol;
DOI:10.1016/j.tet.2013.10.082