C₁₀H₁₄FN₃S

Base Information

Chemical Name:C₁₀H₁₄FN₃S
CAS No.:1248504-07-5
Molecular Formula:C₁₀H₁₄FN₃S
Molecular Weight:227.306
Hs Code.:

C<sub>10</sub>H<sub>14</sub>FN<sub>3</sub>S

Synonyms:C₁₀H₁₄FN₃S

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Chemical Property of C₁₀H₁₄FN₃S

Chemical Property:

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Technology Process of C₁₀H₁₄FN₃S

There total 10 articles about C₁₀H₁₄FN₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1248504-06-4
C₁₅H₂₂FN₃O₂S

: 1248504-07-5
C₁₀H₁₄FN₃S

Guidance literature:: C₁₅H₂₂FN₃O₂S; With trifluoroacetic acid; In chloroform; at 20 ℃; for 1.33333h;

With sodium hydrogencarbonate; In chloroform; water; ethyl acetate;

Reference yield:

: 79110-05-7
1-(2-fluoro-5-nitrophenyl)ethanone

: 1248504-07-5
C₁₀H₁₄FN₃S

Guidance literature:: Multi-step reaction with 10 steps

1: water; ammonium chloride; iron / ethanol; tetrahydrofuran / 2 h / 20 - 70 °C

2: dmap; triethylamine / dichloromethane / 20 °C

3: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

4: triethylamine / dichloromethane / 1.5 h / 20 °C

5: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

6: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

7: tetrahydrofuran / 0.5 h / 20 °C

8: sodium hydroxide; water / methanol / 0.42 h / 50 °C

9: acetonitrile / 3 h / 60 °C

10: trifluoroacetic acid / chloroform / 1.33 h / 20 °C

With dmap; sodium tetrahydroborate; sodium azide; water; iron; ammonium chloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 386216-31-5
(3-acetyl-4-fluorophenyl)carbamic acid tert-butyl ester

: 1248504-07-5
C₁₀H₁₄FN₃S

Guidance literature:: Multi-step reaction with 8 steps

1: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

2: triethylamine / dichloromethane / 1.5 h / 20 °C

3: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

4: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

5: tetrahydrofuran / 0.5 h / 20 °C

6: sodium hydroxide; water / methanol / 0.42 h / 50 °C

7: acetonitrile / 3 h / 60 °C

8: trifluoroacetic acid / chloroform / 1.33 h / 20 °C

With sodium tetrahydroborate; sodium azide; water; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;