(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

Base Information

Chemical Name:(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one
CAS No.:213330-41-7
Molecular Formula:C₂₄H₂₈O₇
Molecular Weight:428.482
Hs Code.:

Synonyms:(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

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Chemical Property of (4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

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Technology Process of (4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

There total 1 articles about (4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 130543-42-9
hept-2-ene-1,7-bisbenzyloxy-4,5,6-triol 4,5-carbonate

: 107-30-2
chloromethyl methyl ether

: 213330-41-7
(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(98)01130-7

Reference yield: 86.0%

: 213330-41-7
(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

: 213330-43-9
(2R,3S,4R)-1-Benzyloxy-2-methoxymethoxy-hept-6-ene-3,4-diol

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; Heating;
DOI:10.1016/S0040-4039(98)01130-7

Reference yield:

: 213330-41-7
(4S,5R)-4-((R)-2-Benzyloxy-1-methoxymethoxy-ethyl)-5-((E)-3-benzyloxy-propenyl)-[1,3]dioxolan-2-one

: (4R,5S)-4-Allyl-5-((R)-2-benzyloxy-1-methoxymethoxy-ethyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / sodium bis(2-methoxyethoxy)aluminium hydride (Red-Al) / toluene / Heating

2: PPTS / CH₂Cl₂

With pyridinium p-toluenesulfonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(98)01130-7