(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

Base Information

Chemical Name:(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal
CAS No.:802552-10-9
Molecular Formula:C₁₂H₁₅NO₃
Molecular Weight:221.256
Hs Code.:

Synonyms:(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

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Technology Process of (2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

There total 9 articles about (2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5153-67-3
nitrostyrene

: 123-72-8
butyraldehyde

: 802552-10-9
(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

: 384354-59-0
(2R,3S)-2-ethyl-4-nitro-3-phenylbutyraldehyde

Guidance literature:: With 4-nitro-phenol; In dichloromethane; at 20 ℃; for 1.5h; stereoselective reaction;
DOI:10.1021/acscatal.5b01746

Reference yield: 95.0%

: 5153-67-3
nitrostyrene

: 123-72-8
butyraldehyde

: 802552-10-9
(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

: (2S,3R)-2-ethyl-4-nitro-3-phenylbutanal

Guidance literature:: With 4-methyl-morpholine; H-_DPro-(4S)Hyp-Glu-NH_{2 *}TFA_;Hyp=hydroxyproline; In chloroform; isopropyl alcohol; at 20 ℃; for 24h; stereoselective reaction;
DOI:10.1055/s-0037-1609547

Reference yield: 92.0%

: 102-96-5
(2-nitroethenyl)benzene

: 123-72-8
butyraldehyde

: 802552-10-9
(2RS,3RS)-2-ethyl-4-nitro-3-phenylbutanal

: (2S,3R)-2-ethyl-4-nitro-3-phenylbutanal

Guidance literature:: With (S)-1-(D-prolyl)-N-((S)-1-phenyl-3-((trifluoromethyl)sulfonamido)propan-2-yl)pyrrolidine-2-carboxamide; benzoic acid; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 24h; stereoselective reaction;
DOI:10.1016/j.tet.2021.132095