4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

Base Information

Chemical Name:4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride
CAS No.:1470142-34-7
Molecular Formula:C₁₀H₉ClFNO₄S
Molecular Weight:293.703
Hs Code.:

Synonyms:4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

Chemical Property:

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Technology Process of 4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

There total 1 articles about 4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.5%

: 1470142-33-6
(4S,5R)-4-(fluoromethyl)-5-phenyloxazolidin-2-one

: 1470142-34-7
4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

Guidance literature:: With chlorosulfonic acid; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1002/jlcr.3053

Reference yield:

: 1470142-34-7
4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

: 73231-34-2
Florfenicol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium sulfite; sodium hydrogencarbonate / water / 70 °C

1.2: 6 h / -45 - 40 °C / Sealed tube; Inert atmosphere

2.1: sulfuric acid / 1,4-dioxane / 0 - 120 °C / Sealed tube

3.1: triethylamine / methanol / 45 °C

With sulfuric acid; sodium hydrogencarbonate; triethylamine; sodium sulfite; In 1,4-dioxane; methanol; water;
DOI:10.1002/jlcr.3053

Reference yield:

: 1470142-34-7
4-((4S,5R)-4-(fluoromethyl)-2-oxooxazolidin-5-yl)benzene-1-sulfonyl chloride

: 76639-93-5,105182-37-4,118015-48-8
(1R,2S)-2-amino-3-fluoro-1-<4-(methylsulphonyl)phenyl>-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium sulfite; sodium hydrogencarbonate / water / 70 °C

1.2: 6 h / -45 - 40 °C / Sealed tube; Inert atmosphere

2.1: sulfuric acid / 1,4-dioxane / 0 - 120 °C / Sealed tube

With sulfuric acid; sodium hydrogencarbonate; sodium sulfite; In 1,4-dioxane; water;
DOI:10.1002/jlcr.3053